TA Instruments

AR1720-0001f

04/09/2012 18:13:13

Sample name	ASW 10 mm from base, 60 mm to top, disk 22 Provil novo maximum texture 
Sample notes	 
Experiment notes	Plastic parallel plate with adaptor supplied by Southampton Uni., on ETC rod with grub screws.

Distances fromlower surface of PP plate. Southampton container.
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1720
Run number	1 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	04/09/2012 18:13:13

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	22.4 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:01:00 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:00:30 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	22.4 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	3.100 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.262 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	3
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	18.42 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

-8.798	7.853	-1.120	0.99600	22.4	1924	5.5099	10000	0.4723	31.20	6.8874	688.74	3.383E-3	0.0	1.0	60.996	-26.993	6.283
0.7948	12.31	0.06459	1.9960	22.4	1938	13.2249	10000	0.4756	12.80	16.531	1653.1	3.384E-3	0.0	1.0	61.996	2.4385	9.845
1.648	19.35	0.08517	3.0000	22.4	1940	26.9091	10000	0.4762	5.181	33.636	3363.6	3.384E-3	0.1	1.1	63.000	5.0568	15.48
2.275	23.03	0.09878	4.0120	22.4	1943	40.8693	10000	0.4770	3.663	51.087	5108.7	3.383E-3	0.1	1.1	64.012	6.9804	18.43
3.902	30.85	0.1265	4.9960	22.4	1943	67.8683	10000	0.4768	2.041	84.835	8483.5	3.383E-3	0.1	1.1	64.996	11.971	24.68
6.388	39.48	0.1618	5.9920	22.4	1948	106.6770	10000	0.4780	1.250	133.35	13335	3.384E-3	0.1	1.1	65.992	19.597	31.58
7.020	42.53	0.1651	6.9960	22.4	1961	126.2910	10000	0.4813	1.084	157.86	15786	3.384E-3	0.1	1.1	66.996	21.538	34.02
9.166	49.13	0.1866	7.9960	22.4	1934	165.2710	10000	0.4746	0.8012	206.59	20659	3.384E-3	0.1	1.1	67.996	28.122	39.30
11.61	57.54	0.2018	8.9960	22.4	1933	223.4420	10000	0.4744	0.5837	279.30	27930	3.384E-3	0.1	1.1	68.996	35.630	46.03
13.53	63.70	0.2124	9.9960	22.4	1924	274.7520	10000	0.4723	0.4743	343.44	34344	3.383E-3	0.2	1.2	69.996	41.502	50.96
15.78	69.65	0.2266	11.000	22.4	1933	326.3490	10000	0.4744	0.3984	407.94	40794	3.383E-3	0.2	1.2	71.000	48.424	55.72
18.07	75.12	0.2405	12.012	22.4	1919	377.1920	10000	0.4711	0.3401	471.49	47149	3.384E-3	0.2	1.2	72.012	55.439	60.10
20.30	80.51	0.2522	12.996	22.4	1915	434.7510	10000	0.4701	0.2955	543.44	54344	3.384E-3	0.2	1.2	72.996	62.286	64.41
22.95	86.44	0.2655	14.004	22.4	1930	498.6450	10000	0.4737	0.2584	623.31	62331	3.384E-3	0.2	1.2	74.004	70.394	69.15
26.43	94.60	0.2794	14.996	22.4	1911	594.7170	10000	0.4691	0.2135	743.40	74340	3.384E-3	0.2	1.2	74.996	81.081	75.68
28.90	99.91	0.2893	15.996	22.4	1915	664.2910	10000	0.4701	0.1919	830.36	83036	3.384E-3	0.3	1.3	75.996	88.668	79.93
32.00	105.7	0.3029	17.000	22.4	1910	740.6630	10000	0.4687	0.1710	925.83	92583	3.384E-3	0.3	1.3	77.000	98.182	84.53
36.26	113.7	0.3188	18.000	22.4	1875	856.2280	10000	0.4602	0.1449	1070.3	1.0703E5	3.383E-3	0.3	1.3	78.000	111.24	90.99
39.00	118.8	0.3283	18.996	22.4	1885	931.1770	10000	0.4626	0.1336	1164.0	1.1640E5	3.383E-3	0.3	1.3	78.996	119.66	95.04
41.68	124.3	0.3354	19.996	22.4	1886	1020.1200	10000	0.4628	0.1221	1275.2	1.2752E5	3.384E-3	0.3	1.3	79.996	127.87	99.40
46.22	132.3	0.3494	21.016	22.4	1886	1153.3900	10000	0.4628	0.1078	1441.7	1.4417E5	3.384E-3	0.4	1.4	81.016	141.80	105.8
49.18	137.4	0.3580	21.992	22.4	1861	1242.1700	10000	0.4567	0.09860	1552.7	1.5527E5	3.384E-3	0.4	1.4	81.992	150.89	109.9
52.31	142.8	0.3663	23.016	22.4	1879	1343.6300	10000	0.4612	0.09214	1679.5	1.6795E5	3.383E-3	0.4	1.4	83.016	160.48	114.2
56.98	150.8	0.3778	24.000	22.4	1849	1495.7100	10000	0.4539	0.08130	1869.6	1.8696E5	3.384E-3	0.4	1.4	84.000	174.82	120.7
60.90	155.9	0.3906	25.020	22.4	1843	1597.1000	10000	0.4522	0.07579	1996.4	1.9964E5	3.384E-3	0.4	1.4	85.020	186.84	124.7
64.33	161.3	0.3988	26.016	22.4	1848	1711.1200	10000	0.4535	0.07099	2138.9	2.1389E5	3.384E-3	0.4	1.4	86.016	197.37	129.1
69.21	169.3	0.4087	27.008	22.4	1807	1886.8700	10000	0.4435	0.06303	2358.6	2.3586E5	3.383E-3	0.5	1.5	87.008	212.33	135.5
72.92	174.4	0.4180	28.012	22.4	1824	1995.9200	10000	0.4476	0.05993	2494.9	2.4949E5	3.384E-3	0.5	1.5	88.012	223.70	139.6
76.89	179.6	0.4282	28.996	22.4	1815	2116.0901	10000	0.4455	0.05630	2645.1	2.6451E5	3.383E-3	0.5	1.5	88.996	235.90	143.6
82.17	187.6	0.4381	30.020	22.4	1811	2305.8501	10000	0.4445	0.05149	2882.3	2.8823E5	3.384E-3	0.5	1.5	90.020	252.10	150.0
85.62	192.7	0.4443	30.996	22.4	1798	2432.3799	10000	0.4413	0.04842	3040.5	3.0405E5	3.384E-3	0.5	1.5	90.996	262.67	154.2
90.64	197.8	0.4582	31.996	22.4	1793	2565.2200	10000	0.4401	0.04581	3206.5	3.2065E5	3.384E-3	0.5	1.5	91.996	278.07	158.3
97.40	205.8	0.4732	33.000	22.4	1782	2774.5901	10000	0.4374	0.04207	3468.2	3.4682E5	3.384E-3	0.6	1.6	93.000	298.83	164.7
101.8	211.0	0.4823	34.016	22.4	1786	2912.8501	10000	0.4384	0.04013	3641.1	3.6411E5	3.383E-3	0.6	1.6	94.016	312.21	168.8
107.4	218.6	0.4914	34.996	22.4	1738	3129.1001	10000	0.4265	0.03636	3911.4	3.9114E5	3.384E-3	0.6	1.6	94.996	329.58	174.9
111.0	223.9	0.4957	35.996	22.4	1751	3279.2000	10000	0.4297	0.03492	4099.0	4.0990E5	3.384E-3	0.6	1.6	95.996	340.50	179.1
115.7	229.1	0.5049	36.996	22.4	1738	3430.8799	10000	0.4267	0.03313	4288.6	4.2886E5	3.384E-3	0.6	1.6	96.996	354.82	183.3
122.5	236.6	0.5176	38.000	22.4	1729	3658.2100	10000	0.4242	0.03087	4572.8	4.5728E5	3.384E-3	0.6	1.6	98.000	375.80	189.3
126.8	241.8	0.5242	38.996	22.4	1737	3823.2900	10000	0.4263	0.02970	4779.1	4.7791E5	3.384E-3	0.6	1.6	98.996	388.95	193.5
133.6	249.6	0.5354	39.996	22.4	1715	4069.6399	10000	0.4210	0.02754	5087.1	5.0871E5	3.384E-3	0.7	1.7	99.996	409.99	199.7
138.7	254.6	0.5446	41.012	22.4	1724	4232.7998	10000	0.4230	0.02659	5291.0	5.2910E5	3.384E-3	0.7	1.7	101.012	425.40	203.7
143.2	259.8	0.5513	41.996	22.4	1696	4500.9199	10000	0.4163	0.02512	5626.2	5.6262E5	3.384E-3	0.7	1.7	101.996	439.48	207.9
150.4	267.6	0.5620	43.000	22.4	1684	4680.6099	10000	0.4133	0.02351	5850.8	5.8508E5	3.384E-3	0.7	1.7	103.000	461.46	214.1
156.2	272.7	0.5728	44.000	22.4	1668	4852.1899	10000	0.4094	0.02244	6065.2	6.0652E5	3.383E-3	0.7	1.7	104.000	479.15	218.1
162.5	280.4	0.5798	45.016	22.4	1645	5129.0498	10000	0.4038	0.02093	6411.3	6.4113E5	3.383E-3	0.8	1.8	105.016	498.68	224.3
168.2	285.5	0.5890	46.024	22.4	1656	5318.4302	10000	0.4064	0.02031	6648.0	6.6480E5	3.383E-3	0.8	1.8	106.024	515.97	228.4
177.7	293.1	0.6064	46.996	22.4	1648	5602.2500	10000	0.4046	0.01918	7002.8	7.0028E5	3.383E-3	0.8	1.8	106.996	545.29	234.5
180.9	298.1	0.6068	47.996	22.4	1642	5797.8701	10000	0.4029	0.01847	7247.3	7.2473E5	3.383E-3	0.8	1.8	107.996	555.01	238.5
184.1	303.4	0.6067	48.996	22.4	1617	6000.9399	10000	0.3969	0.01757	7501.2	7.5012E5	3.383E-3	0.8	1.8	108.996	564.68	242.7
193.9	311.0	0.6236	50.008	22.4	1609	6302.4199	10000	0.3950	0.01664	7878.0	7.8780E5	3.384E-3	0.8	1.8	110.008	594.90	248.8
200.4	316.0	0.6342	50.996	22.4	1593	6510.5698	10000	0.3910	0.01595	8138.2	8.1382E5	3.384E-3	0.8	1.8	110.996	614.85	252.8
209.3	323.8	0.6465	51.996	22.4	1567	6832.4199	10000	0.3845	0.01494	8540.5	8.5405E5	3.384E-3	0.9	1.9	111.996	642.20	259.0
212.1	328.9	0.6449	52.996	22.4	1582	7046.6802	10000	0.3883	0.01463	8808.4	8.8084E5	3.384E-3	0.9	1.9	112.996	650.67	263.1
220.6	336.4	0.6557	53.996	22.4	1547	7374.5898	10000	0.3798	0.01367	9218.2	9.2182E5	3.384E-3	0.9	1.9	113.996	676.74	269.1
225.5	341.6	0.6602	55.012	22.4	1563	7601.6299	10000	0.3837	0.01340	9502.0	9.5020E5	3.383E-3	0.9	1.9	115.012	691.94	273.3
233.1	346.7	0.6724	56.012	22.4	1498	7828.7500	10000	0.3676	0.01246	9785.9	9.7859E5	3.383E-3	0.9	1.9	116.012	715.23	277.4
241.5	354.2	0.6818	57.012	22.4	1478	8169.0200	10000	0.3628	0.01178	10211	1.0211E6	3.383E-3	1.0	2.0	117.012	740.94	283.4
246.7	359.3	0.6866	58.012	22.4	1486	8408.6602	10000	0.3648	0.01151	10511	1.0511E6	3.384E-3	1.0	2.0	118.012	756.95	287.5
259.1	367.0	0.7061	58.996	22.4	1466	8769.9297	10000	0.3597	0.01088	10962	1.0962E6	3.384E-3	1.0	2.0	118.996	795.01	293.6
265.4	372.0	0.7135	60.000	22.4	1519	9007.4600	10000	0.3729	0.01098	11259	1.1259E6	3.383E-3	1.0	2.0	120.000	814.34	297.6

Peak hold step

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

268.3	375.0	0.7155	1.0000	22.4	1472	285.4830	10000	0.3613	0.01047	356.85	35685	3.384E-3	0.0	2.0	122.000	823.15	300.0
269.1	375.0	0.7176	2.0040	22.4	1461	537.2250	10000	0.3585	0.01039	671.53	67153	3.384E-3	0.0	2.1	123.004	825.61	300.0
269.2	375.0	0.7179	2.9960	22.4	1438	915.2550	10000	0.3530	0.01023	1144.1	1.1441E5	3.384E-3	0.0	2.1	123.996	825.93	300.0
268.4	375.0	0.7157	3.9960	22.4	1452	1165.0601	10000	0.3565	0.01033	1456.3	1.4563E5	3.384E-3	0.1	2.1	124.996	823.44	300.0
265.8	375.0	0.7088	4.9960	22.4	1428	1416.2600	10000	0.3506	0.01016	1770.3	1.7703E5	3.384E-3	0.1	2.1	125.996	815.47	300.0
267.6	375.0	0.7137	6.0120	22.4	1452	1795.2900	10000	0.3565	0.01033	2244.1	2.2441E5	3.384E-3	0.1	2.1	127.012	821.12	300.0
270.8	375.0	0.7223	7.0040	22.4	1493	2044.7700	10000	0.3664	0.01062	2556.0	2.5560E5	3.384E-3	0.1	2.1	128.004	830.93	300.0
266.0	375.0	0.7094	8.0120	22.4	1396	2424.9900	10000	0.3427	9.928E-3	3031.2	3.0312E5	3.384E-3	0.1	2.2	129.012	816.12	300.0
265.0	375.0	0.7068	8.9960	22.4	1481	2672.9800	10000	0.3634	0.01053	3341.2	3.3412E5	3.384E-3	0.1	2.2	129.996	813.16	300.0
269.6	375.0	0.7190	10.008	22.4	1462	2926.4299	10000	0.3589	0.01040	3658.0	3.6580E5	3.384E-3	0.2	2.2	131.008	827.18	300.0
265.3	375.0	0.7074	10.996	22.4	1393	3301.3000	10000	0.3419	9.905E-3	4126.6	4.1266E5	3.384E-3	0.2	2.2	131.996	813.87	300.0
273.4	375.0	0.7290	12.008	22.4	1458	3552.5400	10000	0.3579	0.01037	4440.7	4.4407E5	3.383E-3	0.2	2.2	133.008	838.70	300.0
267.7	375.0	0.7139	12.996	22.4	1431	3805.8501	10000	0.3512	0.01018	4757.3	4.7573E5	3.384E-3	0.2	2.2	133.996	821.31	300.0
262.3	375.0	0.6996	13.996	22.4	1437	4182.1401	10000	0.3526	0.01022	5227.7	5.2277E5	3.384E-3	0.2	2.2	134.996	804.84	300.0
266.7	375.0	0.7111	15.000	22.4	1491	4434.2300	10000	0.3660	0.01061	5542.8	5.5428E5	3.383E-3	0.3	2.3	136.000	818.13	300.0
265.3	375.0	0.7073	16.000	22.4	1464	4811.5298	10000	0.3593	0.01041	6014.4	6.0144E5	3.383E-3	0.3	2.3	137.000	813.79	300.0
266.4	375.0	0.7104	17.000	22.4	1451	5060.8799	10000	0.3561	0.01032	6326.1	6.3261E5	3.383E-3	0.3	2.3	138.000	817.24	300.0
266.5	375.0	0.7107	17.996	22.4	1452	5315.7798	10000	0.3563	0.01032	6644.7	6.6447E5	3.383E-3	0.3	2.3	138.996	817.64	300.0
266.2	375.0	0.7098	18.996	22.4	1440	5689.0298	10000	0.3534	0.01024	7111.3	7.1113E5	3.383E-3	0.3	2.3	139.996	816.63	300.0
264.0	375.0	0.7041	19.996	22.4	1463	5940.2798	10000	0.3591	0.01040	7425.4	7.4254E5	3.384E-3	0.3	2.3	140.996	810.08	300.0
265.8	375.0	0.7087	21.000	22.4	1458	6319.3301	10000	0.3579	0.01037	7899.2	7.8992E5	3.384E-3	0.4	2.4	142.000	815.34	300.0
265.2	375.0	0.7072	21.996	22.4	1488	6568.4902	10000	0.3652	0.01058	8210.6	8.2106E5	3.384E-3	0.4	2.4	142.996	813.58	300.0
264.9	375.0	0.7065	22.996	22.4	1492	6820.0098	10000	0.3662	0.01061	8525.0	8.5250E5	3.383E-3	0.4	2.4	143.996	812.85	300.0
265.1	375.0	0.7070	24.012	22.4	1448	7196.8799	10000	0.3555	0.01030	8996.1	8.9961E5	3.383E-3	0.4	2.4	145.012	813.37	300.0
267.7	375.0	0.7138	24.996	22.4	1474	7450.9302	10000	0.3618	0.01048	9313.7	9.3137E5	3.384E-3	0.4	2.4	145.996	821.21	300.0
265.6	375.0	0.7083	26.016	22.4	1419	7699.6001	10000	0.3482	0.01009	9624.5	9.6245E5	3.384E-3	0.4	2.5	147.016	814.90	300.0
268.2	375.0	0.7152	27.108	22.4	1454	8076.5801	10000	0.3569	0.01034	10096	1.0096E6	3.384E-3	0.5	2.5	148.108	822.82	300.0
267.4	375.0	0.7130	28.016	22.4	1465	8327.7803	10000	0.3595	0.01042	10410	1.0410E6	3.383E-3	0.5	2.5	149.016	820.33	300.0
267.5	375.0	0.7134	28.996	22.4	1438	8704.9102	10000	0.3528	0.01022	10881	1.0881E6	3.383E-3	0.5	2.5	149.996	820.80	300.0
264.3	375.0	0.7049	30.020	22.4	1485	8956.2803	10000	0.3644	0.01056	11195	1.1195E6	3.384E-3	0.5	2.5	151.020	810.95	300.0

Continuous ramp step 2

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

262.8	370.7	0.7089	1.0040	22.4	1471	298.9440	10000	0.3611	0.01071	373.68	37368	3.384E-3	0.0	2.6	153.004	806.19	296.5
259.4	365.7	0.7092	2.0080	22.4	1504	534.6770	10000	0.3691	0.01124	668.35	66835	3.383E-3	0.0	2.6	154.008	795.71	292.6
246.3	358.0	0.6878	3.0080	22.4	1453	890.3730	10000	0.3567	0.01134	1113.0	1.1130E5	3.384E-3	0.1	2.6	155.008	755.58	286.4
241.3	352.9	0.6839	4.0080	22.4	1469	1128.2400	10000	0.3605	0.01180	1410.3	1.4103E5	3.384E-3	0.1	2.6	156.008	740.34	282.3
233.0	345.3	0.6749	5.0040	22.4	1524	1471.1600	10000	0.3739	0.01278	1839.0	1.8390E5	3.384E-3	0.1	2.6	157.004	714.95	276.2
228.2	340.2	0.6707	6.0040	22.4	1569	1691.8199	10000	0.3851	0.01355	2114.8	2.1148E5	3.384E-3	0.1	2.6	158.004	700.06	272.2
219.0	335.1	0.6536	7.0080	22.4	1557	1917.2100	10000	0.3820	0.01386	2396.5	2.3965E5	3.384E-3	0.1	2.7	159.008	671.93	268.1
211.2	327.5	0.6447	8.0040	22.4	1623	2236.4800	10000	0.3983	0.01513	2795.6	2.7956E5	3.384E-3	0.1	2.7	160.004	647.84	262.0
204.6	322.5	0.6344	9.0040	22.4	1600	2449.3501	10000	0.3926	0.01538	3061.7	3.0617E5	3.384E-3	0.2	2.7	161.004	627.64	258.0
197.5	314.7	0.6276	10.004	22.4	1630	2772.9199	10000	0.4001	0.01646	3466.2	3.4662E5	3.384E-3	0.2	2.7	162.004	605.93	251.8
193.1	309.7	0.6235	11.000	22.4	1609	2970.9700	10000	0.3948	0.01677	3713.7	3.7137E5	3.384E-3	0.2	2.7	163.000	592.42	247.7
183.7	302.1	0.6082	12.004	22.4	1624	3270.8799	10000	0.3987	0.01780	4088.6	4.0886E5	3.384E-3	0.2	2.7	164.004	563.66	241.7
179.1	296.9	0.6031	13.004	22.4	1639	3469.5000	10000	0.4023	0.01860	4336.9	4.3369E5	3.383E-3	0.2	2.8	165.004	549.34	237.5
174.2	291.7	0.5972	14.004	22.4	1658	3664.5400	10000	0.4070	0.01949	4580.7	4.5807E5	3.383E-3	0.2	2.8	166.004	534.47	233.4
165.9	284.2	0.5837	15.004	22.4	1649	3945.2500	10000	0.4048	0.02042	4931.6	4.9316E5	3.384E-3	0.3	2.8	167.004	508.86	227.3
160.4	279.0	0.5748	16.004	22.4	1692	4132.7002	10000	0.4153	0.02174	5165.9	5.1659E5	3.383E-3	0.3	2.8	168.004	492.01	223.2
153.0	271.2	0.5642	17.052	22.4	1692	4408.0000	10000	0.4153	0.02301	5510.0	5.5100E5	3.384E-3	0.3	2.8	169.052	469.35	216.9
147.0	266.1	0.5523	18.004	22.4	1695	4583.0000	10000	0.4161	0.02394	5728.8	5.7288E5	3.384E-3	0.3	2.8	170.004	450.91	212.9
142.9	261.0	0.5474	19.004	22.4	1684	4758.1299	10000	0.4133	0.02472	5947.7	5.9477E5	3.383E-3	0.3	2.9	171.004	438.29	208.8
136.4	253.2	0.5387	20.004	22.4	1719	5016.8198	10000	0.4220	0.02682	6271.0	6.2710E5	3.384E-3	0.3	2.9	172.004	418.43	202.6
132.0	248.2	0.5321	21.000	22.4	1737	5177.2300	10000	0.4263	0.02820	6471.5	6.4715E5	3.384E-3	0.4	2.9	173.000	405.11	198.5
123.7	240.4	0.5143	22.004	22.4	1748	5420.8999	10000	0.4291	0.03024	6776.1	6.7761E5	3.384E-3	0.4	2.9	174.004	379.38	192.4
120.8	235.2	0.5136	23.008	22.4	1719	5583.5000	10000	0.4218	0.03108	6979.4	6.9794E5	3.384E-3	0.4	2.9	175.008	370.51	188.1
115.8	230.1	0.5031	24.008	22.4	1729	5733.6499	10000	0.4242	0.03266	7167.1	7.1671E5	3.384E-3	0.4	2.9	176.008	355.13	184.1
110.0	222.4	0.4946	25.004	22.4	1745	5961.0498	10000	0.4283	0.03529	7451.3	7.4513E5	3.384E-3	0.4	3.0	177.004	337.42	177.9
105.1	217.1	0.4839	26.004	22.4	1755	6108.5000	10000	0.4307	0.03724	7635.6	7.6356E5	3.383E-3	0.4	3.0	178.004	322.30	173.7
99.20	209.5	0.4735	27.004	22.4	1768	6315.2500	10000	0.4340	0.04029	7894.1	7.8941E5	3.384E-3	0.5	3.0	179.004	304.35	167.6
96.95	204.4	0.4744	28.004	22.4	1767	6452.0801	10000	0.4338	0.04232	8065.1	8.0651E5	3.383E-3	0.5	3.0	180.004	297.44	163.5
91.20	199.1	0.4581	29.004	22.4	1799	6589.4702	10000	0.4415	0.04538	8236.8	8.2368E5	3.384E-3	0.5	3.0	181.004	279.80	159.3
84.14	191.3	0.4399	30.004	22.4	1784	6782.9302	10000	0.4378	0.04875	8478.7	8.4787E5	3.384E-3	0.5	3.0	182.004	258.15	153.0
81.13	186.2	0.4358	31.004	22.4	1815	6907.8901	10000	0.4453	0.05235	8634.9	8.6349E5	3.384E-3	0.5	3.1	183.004	248.90	148.9
77.17	180.9	0.4266	32.004	22.4	1806	7032.7300	10000	0.4433	0.05519	8790.9	8.7909E5	3.383E-3	0.5	3.1	184.004	236.77	144.7
71.47	172.9	0.4134	33.004	22.4	1821	7213.6602	10000	0.4470	0.06094	9017.1	9.0171E5	3.383E-3	0.6	3.1	185.004	219.27	138.3
67.46	167.8	0.4021	34.008	22.4	1845	7325.9102	10000	0.4529	0.06555	9157.4	9.1574E5	3.383E-3	0.6	3.1	186.008	206.97	134.2
62.25	159.8	0.3895	35.004	22.4	1825	7496.2300	10000	0.4480	0.07147	9370.3	9.3703E5	3.384E-3	0.6	3.1	187.004	190.99	127.8
59.18	154.4	0.3832	36.000	22.4	1853	7600.3198	10000	0.4549	0.07770	9500.4	9.5004E5	3.383E-3	0.6	3.1	188.000	181.56	123.6
53.84	146.8	0.3669	37.288	22.4	1861	7750.5898	10000	0.4567	0.08640	9688.2	9.6882E5	3.383E-3	0.6	3.2	189.288	165.18	117.4
50.36	141.4	0.3561	38.004	22.4	1877	7849.5498	10000	0.4608	0.09388	9811.9	9.8119E5	3.383E-3	0.6	3.2	190.004	154.49	113.1
47.63	136.0	0.3501	39.004	22.4	1866	7942.8701	10000	0.4579	0.1008	9928.6	9.9286E5	3.384E-3	0.7	3.2	191.004	146.12	108.8
44.49	131.0	0.3397	40.004	22.4	1876	8030.0801	10000	0.4606	0.1094	10038	1.0038E6	3.383E-3	0.7	3.2	192.004	136.49	104.8
39.27	123.0	0.3192	41.012	22.4	1872	8160.7202	10000	0.4595	0.1237	10201	1.0201E6	3.383E-3	0.7	3.2	193.012	120.48	98.41
36.56	117.4	0.3114	42.000	22.4	1878	8247.7402	10000	0.4610	0.1362	10310	1.0310E6	3.384E-3	0.7	3.2	194.000	112.17	93.93
34.46	112.2	0.3072	43.004	22.4	1898	8322.3203	10000	0.4658	0.1508	10403	1.0403E6	3.383E-3	0.7	3.3	195.004	105.73	89.74
30.09	104.2	0.2888	44.004	22.4	1902	8434.0400	10000	0.4669	0.1752	10543	1.0543E6	3.384E-3	0.7	3.3	196.004	92.315	83.35
27.56	98.50	0.2798	45.004	22.4	1906	8508.7197	10000	0.4679	0.1965	10636	1.0636E6	3.384E-3	0.8	3.3	197.004	84.560	78.80
24.93	93.25	0.2673	46.004	22.4	1909	8570.4600	10000	0.4685	0.2195	10713	1.0713E6	3.384E-3	0.8	3.3	198.004	76.485	74.60
22.38	87.96	0.2545	47.008	22.4	1907	8632.4404	10000	0.4681	0.2465	10791	1.0791E6	3.384E-3	0.8	3.3	199.008	68.674	70.36
20.13	82.33	0.2445	48.004	22.4	1924	8725.9404	10000	0.4723	0.2839	10907	1.0907E6	3.384E-3	0.8	3.3	200.004	61.751	65.86
16.70	74.07	0.2255	49.004	22.4	1926	8774.7100	10000	0.4727	0.3510	10968	1.0968E6	3.384E-3	0.8	3.4	201.004	51.245	59.26
14.56	68.71	0.2119	50.008	22.4	1928	8824.1904	10000	0.4731	0.4083	11030	1.1030E6	3.384E-3	0.8	3.4	202.008	44.661	54.97
12.60	62.92	0.2003	51.008	22.4	1942	8873.1602	10000	0.4766	0.4905	11091	1.1091E6	3.383E-3	0.9	3.4	203.008	38.659	50.34
10.38	56.99	0.1822	52.008	22.4	1936	8934.8096	10000	0.4752	0.5961	11169	1.1169E6	3.384E-3	0.9	3.4	204.008	31.857	45.59
8.298	48.91	0.1697	53.000	22.4	1934	8971.2598	10000	0.4746	0.8083	11214	1.1214E6	3.383E-3	0.9	3.4	205.000	25.457	39.13
6.477	42.74	0.1516	54.004	22.4	1944	9007.6699	10000	0.4772	1.064	11260	1.1260E6	3.384E-3	0.9	3.4	206.004	19.872	34.19
4.875	36.24	0.1345	55.004	22.4	1939	9037.9004	10000	0.4760	1.477	11297	1.1297E6	3.384E-3	0.9	3.5	207.004	14.957	28.99
3.604	30.63	0.1176	56.004	22.4	1951	9061.9600	10000	0.4788	2.079	11327	1.1327E6	3.384E-3	0.9	3.5	208.004	11.057	24.51
2.995	27.44	0.1091	57.008	22.4	1948	9073.9697	10000	0.4780	2.586	11342	1.1342E6	3.384E-3	1.0	3.5	209.008	9.1876	21.95
1.748	19.76	0.08846	58.004	22.4	1943	9096.8301	10000	0.4768	4.977	11371	1.1371E6	3.384E-3	1.0	3.5	210.004	5.3619	15.81
0.8709	13.09	0.06651	59.008	22.4	1944	9108.2803	10000	0.4772	11.34	11385	1.1385E6	3.384E-3	1.0	3.5	211.008	2.6719	10.47
0.4818	9.283	0.05190	60.004	22.4	1927	9115.7803	10000	0.4729	22.36	11395	1.1395E6	3.384E-3	1.0	3.5	212.004	1.4781	7.427

